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This Manual accompanies the Textbook, teaching radioanalytical chemistry to seniors and graduate students. The manual and its accompanying CD-ROM can be used in conjunction with the textbook to teach a 3-hour lecture course and a 6-hour laboratory. The experiments address a range of practical aspects in the radiochemistry laboratory: use of laboratory and radiation detection equipment, performing specific analyses for radio-iodine, radio-strontium, uranium, and plutonium.The education of the radioanalytical chemist has two critical components: theory and practice. The textbook Radioanalytical Chemistry was designed to address the theory component of this education. This laboratory manual accompanies and complements that textbook. This manual provides a framework for the student to hone their laboratory skills, with emphasis on safety, research, experimental design, instrumentation and appropriate laboratory methods.